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Chemistry, 22.06.2019 08:00
Straightforward questions answered in the powerpoint slidesreaction: heating the starting materials under refluxwhat does it mean to heat under reflux? why do we choose water as the reflux solvent? what are boiling chips used for? why do we put a condenser on top of the reaction? why do we add heat and let the reaction stir for 30 minutes? why do we add sulfuric acid to the reaction after it cools as opposed to when it’s still hot? separation: filtration of precipitatewhy don’t we do an aqueous and organic extraction in the separatory funnel? why do you rinse the salicylic acid on the filter with ice cold water? purification: recrystallization of salicylic acid (no hot filtration needed)what is the difference in the amount of room temperature water vs. boiling water needed to dissolve the salicylic acid (assume a 1.2 gram yield of salicylic acid)? remember, in the lab if you need x ml of boiling water to dissolve a solid, then you should add a little more (definitely no more than 1.5 times the theoretical amount) to ensure it doesn’t recrystallize prematurely.analysis: melting point of salicylic acidwhat can you conclude if the melting point of the salicylic acid you just synthesized is 152-155oc and the 1: 1 mix of your product and “synthetic” salicylic acid is 151-154oc?
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Chemistry, 22.06.2019 17:00
Reduction is a reaction which results in a in electrons and a in positive charge of the atom or ion 1) a- loss 1) b- gain 2) a-increase 2) b-decrease
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Chemistry, 23.06.2019 00:30
There are approximately 15 milliliters (ml) in 1 tablespoon (tbsp). what expression can be used to find the approximate number of milliliters in 3 tbsp?
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Chemistry, 23.06.2019 06:00
Jenny wants to test the electrical conductivity of two substances dissolved in water. she is preparing the containers for the experiment. which factor is most important for her to control?
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