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Chemistry, 13.02.2020 21:42 jacobbrandon2002
The concentration of acetylsalicylic acid, C9H8O4, in aspirin tablets is determined by hydrolyzing it to the salicylate ion, C7H5O3-, and determining its concentration spectrofluorometrically. A stock standard solution is prepared by weighing 0.0774 g of salicylic acid, C7H6O3, into a 1-L volumetric flask and diluting to volume. A set of calibration standards is prepared by pipeting 0, 2.00, 4.00, 6.00, 8.00, and 10.00 mL of the stock solution
into separate 100-mL volumetric flasks that contain 2.00 mL of 4 M NaOH and diluting to volume. Fluorescence is measured at an emission wavelength of 400 nm using an excitation wavelength of 310 nm with
results shown in the following table.
Several aspirin tablets are ground to a fine powder in a mortar and pestle. A 0.1013-g portion of the powder is placed in a 1-L volumetric flask and diluted to volume with distilled water. A portion of this solution is filtered to remove insoluble binders and a 10.00-mL aliquot transferred to a 100-mL volumetric flask that contains 2.00 mL of 4 M NaOH. After diluting to volume the fluorescence of the resulting solution is 8.69. What is the %w/w acetylsalicylic acid in the aspirin tablets?
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